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Type: Artigo de Periódico
Title: Comparação estrutural entre amostras de materiais tipo hidrotalcita obtidas a partir de diferentes rotas de síntese
Other Titles: Structural comparison between samples of hydrotalcite-like materials obtained from different synthesis route
Author: Chagas, Luciano H.
Farias, Stephane B. P. de
Leitão, Alexandre A.
Diniz, Renata
Chiaro, Sandra S. X.
Speziali, Nivaldo L.
Abreu, Heitor A. de
Mussel, Wagner N.
Resumo: -
Abstract: Three samples of hydrotalcite-like materials (HTC) were synthesized and their structural characteristics were compared with two HTCs obtained commercially. Thermal analyses, FT-IR, PXRD and textural analyses were used to investigate the structural differences between commercial and synthetic samples. Particularly, the memory effect was observed at temperature higher than 600 ºC. The Rietveld refinements were obtained with expressive accuracy and the statistical parameters of goodness of fit are quite satisfactory. In conclusion, the procedures adopted in synthesis of HTC produced crystalline materials with high surface area materials.
Keywords: Layered double hydroxides
Catalysts supports
Rietveld refinement
CNPq: -
Language: por
Country: Brasil
Publisher: -
Institution Initials: -
Access Type: Acesso Aberto
DOI: http://dx.doi.org/10.1590/S0100-40422012000600008
URI: https://repositorio.ufjf.br/jspui/handle/ufjf/8305
Issue Date: 2012
Appears in Collections:Artigos de Periódicos



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